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As someone who gets nitrogen at the dentist office with a mask I have a theory that it was just him consciously fighting it. It’s positive pressure nitrogen that you just breath in at normal breath rate. If you breath really hard you can displace the nitrogen and suck in some regular air. It sounds like he fought it which caused it to take longer. It is the standard human reaction to fight against one’s own death and I’m guessing he thought that if they held out long enough they would stop. If they are going to use a mask like that as opposed to a hood or chamber they really should sedate the person first.
...this is hilarious. The dentist gives you nitrous oxide (laughing gas), not straight up nitrogen.
The rest of the comment is perfectly valid, though. If I have a mask on my face and I know that it's feeding me a gas that will kill me, I'd do everything I could to dislodge it and hold my breath and whatnot that I could. A far better approach would have been to fill the chamber with nitrogen, ideally without any sort of obvious hissing noise or other tell.
And a far far better approach would have been to not kill the guy in the first place, but I guess there's no stopping that particular bloodlust right now.